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Beilstein J. Org. Chem. 2008, 4, No. 9, doi:10.1186/1860-5397-4-9
Graphical Abstract
Scheme 1: Synthetic route used to prepare vinyl BF3K salts.
Figure 1: Isolated vinyl BF3K salts.
Figure 2: Representative EPR spectra of DBNBS radical adducts obtained during the Te-Li exchange reaction. (A...
Figure 3: Representative EPR spectrum of DBNBS radical adducts obtained during the Li-Boron exchange reaction...
Scheme 2: Experimental conditions. i: 1 equiv nBuLi, Et2O, −78 °C, 30 minutes. ii: 0.8 equiv B(OiPr)3, −20 °C...
Scheme 3: Proposed mechanism of the reaction.